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Undeclared Formaldehyde Levels in Patient Consumer Products The vial was then shaken for 30 seconds and allowed to separate into a toluene layer and aqueous layer. 100 μL of the toluene layer was placed in a 2 mL autosampler vial with a 100 μL glass insert (Restek, Bellefonte, PA). 1 μL of the extract was analyzed by gas chromatography-mass spectrometry (GC/MS) (conditions described below). Common use hplc insert for hplc vials Sigma India 2ml HPLC Vial Insert from Aijiren-Aijiren Hplc Vial...

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