Quantification was done by measuring absorbance of derivates with an Aijiren diode array detector and comparison to standards of known concentrations. The following two elution buffers were used: an aqueous polar phase (1l ultrapure water, 10mM Na 2 HPO 4 , 10mM Na 2 B 4 O 7 , 0.5mM NaN 3 , pH 8.2) and a non-polar phase (0.45 l 99